Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
03 March 2004
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of relevant results.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2004
Report date:
2004

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
(Date of inspection: 02 December 2002 Date of signature: 13 February 2003)
Type of method:
differential scanning calorimetry

Test material

Reference
Name:
Unnamed
Type:
Constituent
Details on test material:
- Name of test material (as cited in study report): TIPX
- Substance type: Colourless liquid.
- Physical state: Liquid.
- Lot/batch No.: 042028.
- Storage condition of test material: Approximately 4ºC in the dark.

Results and discussion

Boiling point
Boiling pt.:
ca. 486 K
Atm. press.:
103.35 kPa
Decomposition:
yes
Decomp. temp.:
>= 483 - <= 485 K
Remarks on result:
other: boiling point estimated at 486K

Any other information on results incl. tables

Determination 1

Thermal Event

Interpretation

Temperature

ºC

K

Approximate onset of exotherm

Approximate onset of decomposition

183.5

457

Exotherm

Decomposition temperature

210.1

483

Atmospheric pressure: 103.35 kPa

Determination 2

Thermal Event

Interpretation

Temperature

ºC

K

Approximate onset of exotherm

Approximate onset of decomposition

182.5

456

Exotherm

Decomposition temperature

212.3

485

Atmospheric pressure: 103.35 kPa

Applicant's summary and conclusion

Conclusions:
The test material has been determined to decompose at approximately 483 to 485 K at 103.35 kPa. As the test material decomposed, no value for boiling temperature could be determined. A calculated value of boiling temperature gave a result of 486 K.
Executive summary:

The test material was decomposed at approximately 483 to 485 K at 103.35 kPa. Therefore, no value of boiling temperature could be determined by differential scanning calorimetry, using ASTM E537-86, Method A2 of Commission Directive 92/69/EEC. A calculated value of boiling temperature gave a result of 486 K.