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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Between 12 February and 30 March 2012.
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Batch# 9311205/008, expiry date 11.2.2013
Melting / freezing pt.:
373 K
Atm. press.:
1 atm
Decomposition:
yes
Decomp. temp.:
>= 168 - <= 441 °C
Sublimation:
no

Please see Attachment 1 of this Summary for the Results section of the report with Thermograms and thermographic data for ease of reading.

Conclusions:
The melting temperature has been determined to be 100 ± 1 °C (373 ± 1 K). Furthermore, decomposition was observed, starting at 168 °C.
Executive summary:

The determination of the melting point was carried out by differential scanning calorimetry (DSC) using a procedure designed to be compatible with Method A1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995. Conclusion: The melting temperature has been determined to be 100 ± 1 °C (373 ± 1 K).

Description of key information

The melting temperature has been determined to be 100 ± 1 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
100 °C

Additional information