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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions)
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 59: Sieve Analysis
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187: Particle Size Analysis by Laser Diffraction
Principles of method if other than guideline:
Laser Diffraction
GLP compliance:
yes (incl. QA statement)
Remarks:
Hess. Ministerium für Umwelt, Energie, Landwirtschaft und Verbraucherschutz
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution
Percentile:
D10
Mean:
1.9 µm
Remarks on result:
other: Standard deviation not reported
Percentile:
D50
Mean:
6.7 µm
Remarks on result:
other: Standard deviation not reported
Percentile:
D90
Mean:
13.6 µm
Remarks on result:
other: Standard deviation not reported

Laser Diffraction


The test item consists of a fine crystalline structure with bacillary form.


 


For each test series fractions (left axis of the ordinate) and the siftings (right axis of the ordinate) are presented in volume % as a function of the particle size.


 


 


The median particle size L50 (50 % of particle volume with lower particle diameter) deduced from these distributions was:


1st test series:               L50 = 6.66 µm


2nd test series:              L50 = 6.64 µm


The average of the median particle size L50 was 6.7 µm


 


 


The particle size L10 (10 % of particle volume with lower particle diameter) deduced from these distributions was:


1st test series:               L10 = 1.92 µm


2nd test series:              L10 = 1.93 µm


The average of the particle size L10 was 1.9 µm


 


 


The particle size L90 (90 % of particle volume with lower particle diameter) deduced from these distributions was:


1st test series:               L90 = 13.67 µm


2nd test series:              L90 = 13.57 µm


The average of the particle size L90 was 13.6 µm

Description of key information

L10: 1.9 µm
L50: 6.7 µm (median particle size)
L90: 13.6 µm


(OECD 110 and CIPAC MT 187, Laser Diffraction)

Additional information