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Physical & Chemical properties

Melting point / freezing point

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Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Experimental test result conducted as per the OECD 102 test guideline.
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
capillary method
Melting / freezing pt.:
> 316 °C
Atm. press.:
975.6 hPa
Decomposition:
yes
Decomp. temp.:
> 316 - < 326.6 °C
Sublimation:
no
Remarks on result:
other: The test item did not melt until 316 °C, instead decomposed between 31.6.3 to 326.6 °C

The mean decomposition range of hydrogen [4-[4-(diethylamino)-2',4' disulphonatobenzhydrylidene]cyclohexa-2,5-dien-1 ylidene] diethylammonium, sodium salt (CAS No. 129-17-9) was found to be 316.3°C - 326.6°C at 975.6 hPa.

Conclusions:
The melting point determination of test item hydrogen [4-[4-(diethylamino)-2',4' disulphonatobenzhydrylidene]cyclohexa-2,5-dien-1 ylidene]diethylammonium, sodium salt (CAS No. 129-17-9) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point was not observed till 316 oC and beyond this temperature the test item decomposed. Hence, the decomposition range was found to be 316.3°C - 326.6°C at 975.6 hPa
Executive summary:

The melting point determination of test item hydrogen [4-[4-(diethylamino)-2',4' disulphonatobenzhydrylidene]cyclohexa-2,5-dien-1 ylidene]diethylammonium, sodium salt (CAS No. 129-17-9) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point was not observed till 316 oC and beyond this temperature the test item decomposed. Hence, the decomposition range was found to be 316.3°C - 326.6°C at 975.6 hPa

Description of key information

The melting point determination of test item hydrogen [4-[4-(diethylamino)-2',4' disulphonatobenzhydrylidene]cyclohexa-2,5-dien-1 ylidene]diethylammonium, sodium salt (CAS No. 129-17-9) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point was not observed till 316 oC and beyond this temperature the test item decomposed. Hence, the decomposition range was found to be 316.3°C - 326.6°C at 975.6 hPa

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
316 °C

Additional information

The melting point determination of test item hydrogen [4-[4-(diethylamino)-2',4' disulphonatobenzhydrylidene]cyclohexa-2,5-dien-1 ylidene]diethylammonium, sodium salt (CAS No. 129-17-9) was done as per the test guideline OECD 102. The method followed was according to Capillary/metal block. The melting point was not observed till 316 oC and beyond this temperature the test item decomposed. Hence, the decomposition range was found to be 316.3°C - 326.6°C at 975.6 hPa