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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
8.11.2019 until 19.3.2020
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Identification: 2-Amino-5-chloro-N,3-dimethylbenzamide
Batch: 628-042-00
CAS number: NA
Purity: 99,0%
Analysis date: 16 October 2019
Expiry date: 16 October 2021
Supplier: ADAMA Makhteshim Ltd.
Appearance: Beige powder
Packaging: White opaque plastic bag
Storage: In darkness at room temperature
Identification: number 19-193
Key result
Melting / freezing pt.:
ca. 144.3 °C
Conclusions:
The mean melting point of the test item was 144.3 °C ± 0.5 °C.
Executive summary:

The melting point fo 2-amino-5-chloro-N,3-dimethylbenzamide was determined according to OECD 102 using Differential Scanning Calorimetry (DSC) to 144.3 °C.

Description of key information

The melting point fo 2-amino-5 -chloro-N,3 -dimethylbenzamide was determined according to OECD 102 and EC A.1 using Differential Scanning Calorimetry (DSC) to 144.3 °C.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
144.3 °C

Additional information