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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
19/04/2017 - 31/05/2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
comparable to guideline study
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Other quality assurance:
other: ISO14001:2004 + Cor1:2009 Enviromental Management System ISO 9001:2008 Quality Management System
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
< -80 °C
Atm. press.:
ca. 1 013 mBar
Decomposition:
no
Conclusions:
The DSC analysis on four different production samples showed a good repeatability and reproducibility anyway there is not evidence of thermal effects. It is possible to exclude a solid-liquid transition in the range between -80°C and + 25°C

Description of key information

According to COLUMN 2 SPECIFIC RULES FOR ADAPTATION FROM COLUMN 1, the Melting/freezing point study does not need to be conducted below a lower limit of - 20 °C.

According to the DSC analysis it is possible to exclude a solid-liquid transition in the range between -80°C and + 25°C.

As surrogate for hazard and risk assessment, freezing point of 1-butanol (-90°C) is considered.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-90 °C

Additional information

Key value exclusively used for hazard and risk assessment purposes.