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Diss Factsheets

Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
May 2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7220 (Boiling Point / Boiling Range)
Version / remarks:
August 1996
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Remarks:
Toxi-Coop ZRT. Arácsi út 97. 8230 Balatonfüred Hungary
Type of method:
differential scanning calorimetry
Key result
Atm. press.:
1 013 hPa
Decomposition:
yes
Decomp. temp.:
<= 500 °C
Remarks on result:
other: The boiling point of Sodium (2-butoxyethoxy) acetate was not observed from room temperature up to 500 °C, but decomposition up to 500 °C.

Appearance of the Samples

Before the test the appearance of Sodium (2-butoxyethoxy) acetate was light yellow, viscous liquid. After the experiments the test item blackened and its volume increased in the crucible.

 

Measurement

The evaluation of the data was performed using the software STARe. As result, a thermogram was obtained in which the heat flow of the investigated sample is given as a function of the temperature. By integrating the area under the heat flow signals, the enthalpy of the process was obtained. During the heating the test item showed endothermic signals in the temperature range of approx. 100 - 170 °C what can be associated with the evaporation of test item.

Table 1. Data of weight and weight loss of the DSC run in the first experiment

Sample weight [mg]

Total loss of mass [%]

Atmospheric Pressure before the measurement (kPa)

18.72

56.3

99.95

 

Table 2. Data of weight and weight loss of the DSC run in the second experiment

Sample weight [mg]

Total loss of mass [%]

Atmospheric Pressure before the measurement (kPa)

13.63

56.3

99.95

Conclusions:
The test item decomposes up to 500°C.
Executive summary:

A study was performed in accordance with OECD TG 103 in order to determine the boiling point of the test item using the differential scanning calorimetry method. The test was carried out at normal atmospheric pressure. Using a linear heating rate of 10 °C/min the boiling point of Sodium (2-butoxyethoxy) acetate was not observed from room temperature up to 500 °C. Based on the results of the DSC curves and the appearance of test item after the tests, it is concluded the test item decomposes up to 500 °C.

Description of key information

The test item decomposes up to 500°C.

Key value for chemical safety assessment

Additional information

A study was performed in accordance with OECD TG 103 in order to determine the boiling point of the test item using the differential scanning calorimetry method. The test was carried out at normal atmospheric pressure.Using a linear heating rate of 10 °C/min the boiling point of Sodium (2-butoxyethoxy) acetate was not observed from room temperature up to 500 °C. Based on the results of the DSC curves and the appearance of test item after the tests, it is concluded the test item decomposes up to 500 °C.