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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Actual guideline method. GLP.
Cross-reference
Reason / purpose for cross-reference:
reference to other study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
3-[(2-aminoethyl)amino]propane-1-sulfonic acid
Cas Number:
14235-54-2
Molecular formula:
C5H14N2O3S
IUPAC Name:
3-[(2-aminoethyl)amino]propane-1-sulfonic acid
Details on test material:
- Physical state: solid
- Analytical purity: approx. 95 %
- Impurities (identity and concentrations): water approx 5%
- Lot/batch No.: 06060423/101
- Stability under test conditions: stable
- Storage condition of test material: room temperature in the dark

Results and discussion

Melting / freezing point
Melting / freezing pt.:
25 - 150 °C
Atm. press.:
1 atm
Decomposition:
no
Remarks on result:
other: At the start of the test at 25 °C the test substance was a highly viscous non-stirrable mass. The viscosity of the test substance decreased throughout the whole test beginning at 25 °C. At about 150 °C the test substance was a liquid of low viscosity.

Applicant's summary and conclusion

Conclusions:
The experimental determined melting range of the test substance is < 25 °C to 150 °C.
Executive summary:

The melting temperature was determined experimentally using the capillary method of OECD and EC.

At the start of the test at 25 °C the test substance was a highly viscous non-stirrable mass.

The viscosity of the test substance decreased throughout the whole test beginning at 25 °C. At about 150 °C the test substance was a liquid of low viscosity. Due to these observations no melting point but a melting range was stated.

Range:            <25 °C to 150 °C