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Physical & Chemical properties

Flash point

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Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
18 January 2017 to 19 January 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes (incl. certificate)
Type of method:
equilibrium method closed cup
Flash point apparatus:
Setaflash apparatus
Key result
Flash point:
87 °C
Remarks on result:
other: result was corrected for atmospheric pressure

TABLE 1 – RESULTS OF FLASH POINT DETERMINATION

Test temperature (°C)

Observations

21.0

No flash

26.0

No flash

31.0

No flash

36.0

No flash

41.0

No flash

46.0

No flash

51.0

No flash

56.0

No flash

61.0

No flash

66.0

No flash

71.0

No flash

71.0 (fresh sample)

No flash

76.0

No flash

81.0

No flash

86.0

No flash

91.0

A blue/green flash spread across the sample cup

91.0 (fresh sample)

A blue/green flash spread across the sample cup

86.0 (fresh sample)

No flash

87.0 (fresh sample)

A blue/green flash spread across the sample cup

87.0 (fresh sample)

A blue/green flash spread across the sample cup

85.0 (fresh sample)

No flash

85.0 (fresh sample)

No flash

Atmospheric pressure: 103.1kPa

Corrected flash point: 86.6°C

Interpretation of results:
GHS criteria not met
Conclusions:
The flash point of the test item was determined to be 87 ± 2 °C.
Executive summary:

GUIDELINE

The determination was carried out using a closed cup Setaflash 30000-0 flash point tester and was designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

 

RESULTS

The flash point of the test item was determined to be 87 ± 2 °C.

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
13 October 2016 to 16 October 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes (incl. certificate)
Type of method:
equilibrium method closed cup
Flash point apparatus:
Setaflash apparatus
Key result
Remarks on result:
no flash point - measurement carried out until boiling temperature

TABLE 1 – RESULTS OF FLASH POINT DETERMINATION

Test temperature (°C)

Observations

21.0

No flash

26.0

No flash

31.0

No flash

36.0

No flash

41.0

No flash

46.0

No flash

51.0

No flash

56.0

No flash

61.0

No flash

66.0

No flash

71.0

No flash

71.0 (fresh sample)

No flash

76.0

No flash

81.0

No flash

86.0

No flash

91.0

No flash

96.0

No flash

101.0 (fresh sample)

No flash

106.0

No flash

111.0

No flash

116.0

No flash

121.0

No flash

126.0

No flash

131.0

No flash

136.0

No flash

141.0

No flash

146.0

No flash

151.0

No flash

151.0 (fresh sample)

No flash, boiling observed.

146.0 (fresh sample)

No flash, boiling observed.

141.0 (fresh sample)

No flash, boiling observed.

136.0 (fresh sample)

No flash, boiling observed.

131.0 (fresh sample)

No flash, boiling observed.

126.0 (fresh sample)

No flash, boiling observed.

121.0 (fresh sample)

No flash, boiling observed.

116.0 (fresh sample)

No flash, boiling observed.

111.0 (fresh sample)

No flash

112.0 (fresh sample)

No flash

113.0 (fresh sample)

No flash

114.0 (fresh sample)

No flash, boiling observed.

114.0 (fresh sample)

No flash, boiling observed.

112.0 (fresh sample)

No flash

Interpretation of results:
GHS criteria not met
Conclusions:
The test item was determined to have no flash point below its boiling temperature.
Executive summary:

GUIDELINE

The determination was carried out using a closed cup Setaflash 30000-0 flash point tester and was designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

 

RESULTS

The test item was determined to have no flash point below its boiling temperature.

Description of key information

Using the closed cup equilibrium method, the research material was determined to have no flash point below the boiling temperature and the flash point of the manufactured product was determined to be 87 ± 2 °C (EU Method A.9).

Key value for chemical safety assessment

Flash point at 101 325 Pa:
87 °C

Additional information

GUIDELINE

The determinations were carried out using a closed cup Setaflash 30000-0 flash point tester and was designed to be compatible with Method A.9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

RESULTS

Using the closed cup equilibrium method, the research material was determined to have no flash point below the boiling temperature and the flash point of the manufactured product was determined to be 87 ± 2 °C.