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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2014-11-20 to 2014-11-21
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
167.3 °C
Atm. press.:
1 013 hPa
Decomposition:
no

Results of the DSC Measurements:

Measurement no.

Onset of Effect / °C

Range of Effect /°C

Atmospheric pressure / hPA

1

-68.40 – 167.49

 

110-200 (endo)

1007.1

2

--68.21 – 166.95

120-200 (endo)

1007.1

During the heating phase the test item showed an endothermic signal in the temperature range of 110-200°C that can be associated with the boiling point of the test item. The lowest measured onset temperature is corrected to the standard pressure to be 166.93 °C and the highest onset temperature to be 167.72 °C.

As the corrected onset temperatures in both tests deviate by less than 0.5 K from their mean value of 167.33 °C, the test item has a boiling point of 167.3 °C.

No further effects were observed up to 500 °C

Conclusions:
The test item has a boiling point of 167.3 °C corrected to normal atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry.
Executive summary:

The test item has a boiling point of 167.3 °C corrected to normal atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995).

 

Description of key information

Boiling point: 167.3°C at 1013 hPa

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
167.3 °C

Additional information

The test item has a boiling point of 167.3 °C corrected to normal atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995).