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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Melting / freezing pt.:
227.4 °C
Remarks on result:
other: atmospheric pressure

Measurements were done at atmospheric pressure

Sample mass [mg]   Melting point [ °C]
 9.3  227.5
 14.2  227.2
 15.4  227.4
 Mean value  227.4

 

Conclusions:
The melting point was determined as 227.4 °C at atmospheric pressure.
Executive summary:

The test was conducted according to EC test Procedure A.1 'Melting/Freezing Temperature' and ASTM E 537 'Standard method for assessing the thermal stability of chemicals by methods of differential thermal analysis'.

The measurement was done by Differential Scanning Calorimetry. Macrolex Orange R and reference crucible with an inert sample were subjected to the same controlled temperature program. The sample was heated in a glass crucible at a linear rate of 1 K/min from 210 °C up to 240 °C. The measurement was recorded electronically.

The melting point was determined as 227.4 °C at atmospheric pressure.

Description of key information

The test was conducted according to EC test Procedure A.1 'Melting/Freezing Temperature' and ASTM E 537 'Standard method for assessing the thermal stability of chemicals by methods of differential thermal analysis'.

The measurement was done by Differential Scanning Calorimetry. Macrolex Orange R and reference crucible with an inert sample were subjected to the same controlled temperature program. The sample was heated in a glass crucible at a linear rate of 1 K/min from 210 °C up to 240 °C. The measurement was recorded electronically.

The melting point was determined as 227.4 °C at atmospheric pressure.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
227.4 °C

Additional information