Registration Dossier

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
01 December 2008 to 10 March 2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Study conducted to GLP in compliance with agreed protocols with no deviations from standard test guidelines and/or minor methodological deficiences which do not affect the quality of the relevant results

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report Date:
2009

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to
Guideline:
other: ASTM E537-86
Deviations:
no
Qualifier:
according to
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. certificate)
Type of method:
other: Differential Scanning Calorimetry

Test material

Reference
Name:
Unnamed
Type:
Constituent
Details on test material:
- Name of test material (as cited in study report): INK BH11 M
- Structural formula attached as image file (if other than submission substance): see Fig.
- Substance type: dark red powder
- Lot/batch No.: MB-1A
- Storage condition of test material: room temperature in the dark

Results and discussion

Melting / freezing point
Remarks on result:
other: Test material has been determined to decompose from approximately 518 K at 101.6 +/- 0.1 kPa

Any other information on results incl. tables

Test material decomposed at 518 K. Decomposition was confirmed using a modified liquid bath method. On removal from the apparatus, the test material was confirmed as having decomposed into a black solid.

Applicant's summary and conclusion

Conclusions:
The substance was shown to decompose from approximately 518 K at 101.6±0.1 kPa.
Executive summary:

In a determination of general physico-chemical properties study (Harlan project number: 0959/0234) the test material

is shown to decompose from approximately 518 K (245°C) at 101.6 kPa. The determination was carried out by

differential scanning calorimetry (DSC) using the procedures specified in ASTM E537-86 method and Method A1

melting/freezing temperature of commission regulation (EC) No 440/2008 of 30 May 2008. The methods were

undertaken in two different atmospheres, air (static) and nitrogen to give the same decomposition temperature

indicating the decomposition is probably thermal and not oxidative.