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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
from 03 November 2009 to 03 November 2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study with dated and signed quality assurance inspection statement included.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
not specified
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
not specified
GLP compliance:
yes
Type of method:
other: capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
Methanesulphonyl chloride
EC Number:
204-706-1
EC Name:
Methanesulphonyl chloride
Cas Number:
124-63-0
Molecular formula:
CH3ClO2S
IUPAC Name:
methanesulfonyl chloride
Details on test material:
Name: methanesulphonyl chloride
batch n. 096260041
Expiration date: July 2011
Production date: july 2009
Storage: room temperature - darkness
Purity: 99.8%
Manufacturer: OXON Italia S.p.A.
The identification of the test item was made by its appaerance and colour by the LAB Research Ltd.

Results and discussion

Boiling point
Boiling pt.:
159.4 °C
Atm. press.:
96.5 kPa
Decomposition:
no
Remarks on result:
other: 95% confidence interval

Any other information on results incl. tables

The test was carried out at 96.5 kPa atmospheric pressure. Using a linear heating rate of 0.5 °C/min, the boiling point of Methanesulfonyl Chloride was found to be 159.4 ± 0.05 °C (95 % confidence interval), i.e. 432.5 K.

Measured temperatures corresponding to the boiling point of Methanesulfonyl Chloride (three experiments (I, II, III) with two parallel samples each (1, 2):

 

Measured Temperatures during the Main Study (°C)

I/1

I/1

II/1

II/1

III/1

III/1

MEAN

Boiling point

159.4

159.4

159.3

159.3

159.4

159.4

159.4

Applicant's summary and conclusion