Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Study was performed in internal lab using different methods. An OECD study is currently conducted.

Data source

Reference
Reference Type:
other company data
Title:
Unnamed
Year:
2020
Report date:
2020

Materials and methods

Principles of method if other than guideline:
Freezing point was determined with different methods (visual inspection, DSC)
- Cooling down the test substance mixture in a test tube with a cryostat, evaluation of the crystallization point by optical analytics
- Freezing Point Test – visual test using freezer at -50 ℃
- Freezing Point Test with DSC
GLP compliance:
no
Type of method:
other: Freezing point was determined with different methods (visual inspection, DSC)

Test material

Constituent 1
Chemical structure
Reference substance name:
1-Ethyl-3-methylimidazolium Diethyl Phosphate
Cas Number:
848641-69-0
Molecular formula:
C6H11N2 C4H10O4P
IUPAC Name:
1-Ethyl-3-methylimidazolium Diethyl Phosphate
Test material form:
liquid
Details on test material:
Batch No 187-9-113-Y
Expiry date: 2021-1-30
Specific details on test material used for the study:
Test substance was investigated with different water content (up to 40%), results can be obtained up to 60 wt.-% of test item

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
-38 < °C

Any other information on results incl. tables

Substance was tested with different water content. Eutectic point was between 60 and 100 wt% test item. No crystallization of the test item was observed due
to very high viscosity. Pure test item  (water content ~ 1-2 %) did not crystallize at – 50 °C, but was highly viscous.

Applicant's summary and conclusion

Conclusions:
The freezing point of the test substance is below -38°C
Executive summary:

The freezing point of the test substance (80 wt%) is below -38°C. Test item containing small amounts of water (water content ~ 1-2 %) did not crystallize at – 50 °C, but was highly viscous and to the blank eye not moving anymore.