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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
25/9/2013 to 13/11/2013
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
no
Type of method:
distillation method
Key result
Boiling pt.:
95.2 °C
Atm. press.:
0.33 kPa
Remarks on result:
other: The test item was not distilled below 270°C, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined at reduced pressure.
Boiling pt.:
368.4 K
Atm. press.:
0.33 kPa
Remarks on result:
other: The test item was not distilled below 543.2 K, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined at reduced pressure.

Table 1 Boiling point at atmospheric pressure (102.0 kPa)

Run

Temperature

Pressure

1

Not Determined

(not distilled below

270.0℃(543.2 K))

102.0 kPa

2

Not Determined

(not distilled below

270.0℃(543.2 K))

102.0 kPa

Table 2 Boiling point at reduced pressure (0.33 kPa)

Run

Temperature

Pressure

1

95.0℃(368.2 K)

0.33 kPa

2

95.3℃(368.5 K)

0.33 kPa

Average

95.2℃(368.4 K)

0.33 kPa
Conclusions:
The test item was not distilled below 270°C, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined to be 95.2°C (368.4 K) at reduced pressure (0.33 kPa), with no reaction or decomposition.
Executive summary:

The boiling point of the test item was measured by using a general distillation apparatus under atmospheric pressure and at reduced pressure. Two runs were made, and OECD guideline 103 was followed. The test item was not distilled below 270°C, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined to be 95.2°C (368.4 K) at reduced pressure (0.33 kPa), with no reaction or decomposition.

Description of key information

The test item was not distilled below 270°C, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined to be 95.2°C (368.4 K) at reduced pressure (0.33 kPa), with no reaction or decomposition.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
270 °C

Additional information

The boiling point of the test item was measured by using a general distillation apparatus under atmospheric pressure and at reduced pressure (2014). Two runs were made, and OECD guideline 103 was followed. The test item was not distilled below 270°C, with no reaction or decomposition, at atmospheric pressure. Boiling point could not be measured at atmospheric pressure (102.0 kPa). Boiling point was determined to be 95.2°C (368.4 K) at reduced pressure (0.33 kPa), with no reaction or decomposition.

The study is a guideline experimental study, and is reliable without restrictions (Klimisch 1).