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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: well performed study according to internal rules

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: company SOP
Principles of method if other than guideline:
Determination of the melting point by DSC:
Apparatus: Mettler Toledo, DSC 823e
Conditions: 25 – 300°C, 10 K/min, aluminium pan with hole
GLP compliance:
no
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
3-amino-N-(4-carbamoylphenyl)-4-methoxybenzamide hydrochloride
EC Number:
618-990-3
Cas Number:
939961-06-5
Molecular formula:
C15H15N3O3xClH
IUPAC Name:
3-amino-N-(4-carbamoylphenyl)-4-methoxybenzamide hydrochloride
Details on test material:
Purity: 94.7 % (w/w)

Results and discussion

Melting / freezing point
Melting / freezing pt.:
270 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
ca. 277 °C
Sublimation:
no

Applicant's summary and conclusion

Conclusions:
The melting point of the substance is 270 °C.
Executive summary:

Detemination of the melting point was performed via DSC with a Mettler Toledo, DSC 823e. The heating rate was 10 K/min and the the substance was capsuled in an aluminum pan with hole. The melting point was found to be 270 °C