Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

Currently viewing:

Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
1992
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
215 °C
Atm. press.:
ca. 1 013.25 hPa

Three measurements in aluminium crucibles with a hole showed an endothermic effect after themelting in the temperature range 180 - 230 °C with an onset temperature of 214 °C. For the correction At of the boiling point to standard atmospheric pressure (1013.3 hPa) the equation,table and graphs of H.B. Mass and R.F. Newton in ,,CRC Handbook of Chemistry and Physics, 74thed. 1993-1994", pages 15-16 and 15-17 were used. At = [(273.15+t) (3.0057-log p)] / [O + 0.15(3.0057-log p)](t in °C, p in hPa)


 


Validity criteria for the measurement of the boiling point:




















Target condition according to guideline OECD 103:Actual condition according to the study:Validity criteria met:
The mean of at least two measurements which are in the range of the estimated accuracy (DSC = +/- 0.5 K) should be reported.

Three measurements were performed. The onset temperature values obtained were 214.46 +/- 0.89 °C. The small temperature variation above 0.5 °C is acceptable as three measurements were perfomerd.


Yes
The pressure(s) at which the measurements were made shall be reported. The pressure should preferably be close to normal atmospheric pressure.The atmospheric pressure is stated for each value and was close to normal in each test.Yes

 

Conclusions:
The test item has a boiling point at atmospheric pressure of 215 °C.
Executive summary:

The test item has a boiling point at atmospheric pressure of 215 °C.

Description of key information

The test item has a boiling point at atmospheric pressure of 215 °C.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
215 °C

Additional information