N,N-diethylaniline

Melting point / freezing point

Link to relevant study record(s)

Reference

Endpoint:

melting point/freezing point

Type of information:

experimental study

Adequacy of study:

key study

Study period:

26/02/2016-26/02/2016

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Justification for type of information:

Data is from experimental study report

Qualifier:

according to guideline

Guideline:

other: as mentioned below

Principles of method if other than guideline:

The Freezing point determination of test chemical was done using crushed ice-salt cooling bath.

GLP compliance:

no

Type of method:

other: crushed ice-salt cooling bath.

Key result

Melting / freezing pt.:

< -13.8 °C

Atm. press.:

976.8 hPa

Remarks on result:

other: No other details available

TEST DESCRIPTION AND RESULTS

Method Details		Observations	Remarks if, any
Method	Freezing Temperature Method
Principle of Freezing point test	The freezing point of a pure sample is the temperature at which transition from liquid to solid state takes place at atmospheric pressure.		-
Quantity of test item used	g	1.0
Type of cooling bath used	·        Cold Water ·        Crushed Ice ·        Crushed Ice-Salt ·        Dry Ice ·        Other (specify)	Crushed ice -salt	-
Type and model no. of temperature sensor used	·        Glass thermometer ·        Thermocouple ·        Thermistor ·        Other (specify)	Thermistor model 103	-
Atmospheric pressure	hPa	976.8	-
Freezing point °C	°C	<-13.8	-

Conclusions:

The Freezing point of test chemical was determined with crushed ice-salt cooling bath and the freezing point was inferred to be < -13.8 °C at 976.8 hPa.

Executive summary:

The Freezing point determination of test chemical was done using crushed ice-salt cooling bath. No crystallization was observed up to -13.8°C. Hence, the freezing point was inferred to be<-13.8°C at976.8hPa.

Description of key information

The Freezing point determination of test chemical was done using crushed ice-salt cooling bath. No crystallization was observed up to -13.8°C. Hence, the freezing point was inferred to be<-13.8°C at976.8hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:

-38.8 °C

Additional information

The Freezing point determination of test chemical was done using crushed ice-salt cooling bath. No crystallization was observed up to -13.8°C. Hence, the freezing point was inferred to be<-13.8°C at976.8hPa.

The other reported data from reliable handbook and authoritative database inidcates the freezing point of test chemical as 38.8 degree C.