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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 2021
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2021

Materials and methods

Test guidelineopen allclose all
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
yes
Remarks:
only one measurement was performed; no reference material was subjected to the same controlled temperature programme
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
yes
Remarks:
only one measurement was performed; no reference material was subjected to the same controlled temperature programme
Principles of method if other than guideline:
The test was carried out with a thermal analysis TA Instruments Q600 equipment.

GLP compliance:
no
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
Tricobalt bis(orthophosphate)
EC Number:
236-655-6
EC Name:
Tricobalt bis(orthophosphate)
Cas Number:
13455-36-2
Molecular formula:
Co3(PO4)2
IUPAC Name:
tricobalt bis(orthophosphate)
impurity 1
Chemical structure
Reference substance name:
Dicobalt diphosphate
EC Number:
238-689-7
EC Name:
Dicobalt diphosphate
Cas Number:
14640-56-3
Molecular formula:
Co2P2O7
IUPAC Name:
dicobalt diphosphate
impurity 2
Chemical structure
Reference substance name:
cobalt phosphate octahydrate
Cas Number:
10294-50-5
Molecular formula:
Co3(PO4)2.8H2O
IUPAC Name:
cobalt phosphate octahydrate
Test material form:
solid: particulate/powder

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
>= 800 °C
Sublimation:
no
Remarks on result:
other: no significant thermal effects up to 800°C.

Any other information on results incl. tables

The test item shows an endothermic weight loss early on, about 140°C or so, then gradual minor weight loss thereafter. The minor weight loss above 200°C is less than 0.2 -0.4%. The analysis shows that the test item is stable up to 800°C.

Applicant's summary and conclusion

Conclusions:
The test item has no melting point up to 800 °C. No significant thermal effects from room temperature to 800 °C were determined in a differential thermal analysis.