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Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
26 August - 22 December 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report Date:
2016

Materials and methods

Test guideline
Qualifier:
according to
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Deviations:
no
GLP compliance:
yes

Test material

Reference
Name:
Unnamed
Type:
Constituent
Test material form:
solid: particulate/powder
Details on test material:
- Name of test material (as cited in study reports): JNJ-150098-AAC (T001310)
- Physical state: solid
- Appearance white powder
Specific details on test material used for the study:
- Batch n°: I14KB4913
- Analytical purity: 97.4% (base titration)
- Expiration date: 23 November 2020 (retest date)
- Storage condition: at room temperature

Results and discussion

Relative self-ignition temperature (solids)
Key result
Remarks on result:
no self-ignition observed up to the melting point

Any other information on results incl. tables

A strong exothermic effect of the test item was observed. The temperature of the test item reached 400°C at an oven temperature of 390°C. It demonstrated that the self-ignition temperature of the test item is 390°C.

After the experiment, the test item had turned into a black/brown residue and was partially collected in a container that was placed below the cube. It indicated that the test item had expanded, decomposed and/or reacted during the experiment.

At temperatures below 390°C the sample temperature followed the oven temperature. No self-ignition was observed up to the melting point (298.2°C).

Applicant's summary and conclusion

Conclusions:
In the EC A.16 test performed, the self-ignition temperature of JNJ-150098-AAC (T001310) was determined to be 390°C. At lower oven temperatures, the sample temperature followed the oven temperature. Up to the melting point (298.2°C) no self-ignition was observed.