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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2008-07-03
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: No GLP but guideline compliant study.
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions)
Version / remarks:
ISO 13320-1
Deviations:
no
GLP compliance:
not specified
Type of method:
Laser scattering/diffraction
Percentile:
D50
Mean:
>= 114.83 - <= 115.12 µm
St. dev.:
0.145
Percentile:
D10
Mean:
>= 28.2 - <= 28.89 µm
St. dev.:
0.345
Percentile:
D90
Mean:
>= 262.46 - <= 274.38 µm
St. dev.:
5.96
No.:
#1
Size:
>= 28.2 - <= 28.89 µm
Distribution:
>= 3.94 - <= 4.25 %
No.:
#2
Size:
>= 114.83 - <= 115.12 µm
Distribution:
>= 15.15 - < 15.47 %
No.:
#3
Size:
>= 262.46 - <= 274.38 µm
Distribution:
>= 43.44 - <= 43.61 %
Conclusions:
The particle size of lithium bis(oxalato)borate was analysed by the particle size analyser HELOS. The size and distribution of the particles were analysed as follows:
D10: >= 28.20 - <= 28.89 µm (distribution: >= 3.94 - <= 4.25 %)
D50: >= 114.83 - <= 115.12 µm (distribution: >= 15.15 - <= 15.47 %)
D90: >= 262.45 - <= 274.38 µm (distribution: >= 43.44 - <= 43.61 %)
Executive summary:

The particle size of lithium bis(oxalato)borate was determined according to OECD guideline 110. The particle size of lithium bis(oxalato)borate was analysed by the particle size analyser HELOS (by Sympatec GmbH, Clausthal-Zellerfeld, Germany) and WINDOX 5 software for control of the instruments and evaluation of particle size analysis data.

The size and distribution of the particles were analysed as follows:

D10: >= 28.20 - <= 28.89 µm (distribution: >= 3.94 - <= 4.25 %)

D50: >= 114.83 - <= 115.12 µm (distribution: >= 15.15 - <= 15.47 %)

D90: >= 262.45 - <= 274.38 µm (distribution: >= 43.44 - <= 43.61 %)

(Sympatec, 2008)

Description of key information

The particle size of lithium bis(oxalato)borate was analysed by the particle size analyser HELOS. The size and distribution of the particles were analysed as follows: 
D10: >= 28.20 - <= 28.89 µm (distribution: >= 3.94 - <= 4.25 %)
D50: >= 114.83 - <= 115.12 µm (distribution: >= 15.15 - <= 15.47 %)
D90: >= 262.45 - <= 274.38 µm (distribution: >= 43.44 - <= 43.61 %)

Additional information

The particle size of lithium bis(oxalato)borate was determined according to OECD guideline 110. The particle size of lithium bis(oxalato)borate was analysed by the particle size analyser HELOS (by Sympatec GmbH, Clausthal-Zellerfeld, Germany) and WINDOX 5 software for control of the instruments and evaluation of particle size analysis data.

The size and distribution of the particles were analysed as follows:

D10: >= 28.20 - <= 28.89 µm (distribution: >= 3.94 - <= 4.25 %)

D50: >= 114.83 - <= 115.12 µm (distribution: >= 15.15 - <= 15.47 %)

D90: >= 262.45 - <= 274.38 µm (distribution: >= 43.44 - <= 43.61 %)

(Sympatec, 2008)