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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From November 2001 to January 2002
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
not specified
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
Lot no: MRT-2518-038
Identity: C12-14 ADEBAC
Purity: 68 % C12-alkyl compound, 32 % C14-alkyl compound
Appearance: White solid
Storage: Room temperature, desiccated
Key result
Atm. press.:
1 008 mBar
Decomposition:
yes
Decomp. temp.:
> 140 °C
Remarks on result:
not determinable
Remarks:
The test substance decomposed at temperatures above 140ºC without boiling.
Conclusions:
Under study conditions, boiling point of the test substance was not determinable, as the test substance decomposed at temperatures above 140ºC without boiling (Sydney 2002).
Executive summary:

A study was conducted to determine the boiling point of test substance, C12-14 ADEBAC (active not specified), using modified Siwoloboff method according to the OECD Guideline 103 and EU Method A.3, in compliance with GLP. During the experiment, the test substance was observed to become clear and less viscous before darkening commenced at approximately 140ºC. Heating was continued at 10ºC /minute from 150ºC to 220ºC, and 1ºC/minute thereafter, until the decomposed samples, now light brown in color, boiled at approximately 230ºC. Under study conditions, the boiling temperature of the test substance was not determinable, as the test substance decomposed at temperatures above 140ºC without boiling (Sydney 2002).

Description of key information

The boiling point of test substance was determined using modified Siwoloboff method, according to the OECD Guideline 103 and EU Method A.3 (Sydney, 2002).

Key value for chemical safety assessment

Additional information

Not determinable, as the test substance decomposed >140ºC, without boiling.