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Physical & Chemical properties

Density

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Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2018-01-05 to 2018-02-15
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
other: gas comparison pycnometer
Specific details on test material used for the study:
CAS No.: 17696-62-7
Batch: 018964K19K
Expiry date: 02 August 2018
Purity: 99.1%
Appearance: White powder
Storage: In darkness at room temperature
Key result
Type:
relative density
Density:
1.276 other: no unit
Temp.:
18.7 °C

Assay No. 1:

Test item sample weight (ME): 2.2880 g

Reference volume (VA): 79.444 cm3

Volume of sample cell holder (VC): 27.678 cm3

Temperature during the assay: 18.5 °C

Table 1: Results of assay No. 1 (The run No. 1 was not taken into account as it did not comply with the quality criteria)

 Data

P2 (PSIG)

 

P3 (PSIG)

VP (cm3)

 Density (g/cm3) Relative density   Mean relative density
 Run No. 2  17.076 4.197   1.7888 1.2790 1.2791  

1.279 ± 0.001

    
 Run No. 3  17.136 4.212   1.7868  1.2805

1.2805

 Run No. 4  17.097 4.202  1.7902  1.2781 1.2781

Assay No. 2:

Test item sample weight (ME): 2.6223 g

Reference volume (VA): 79.444 cm3

Volume of sample cell holder (VC): 27.678 cm3

Temperature during the assay: 18.9 °C

Table 2: Results of assay No. 2 (The runs No. 1 and 2 were not taken into account as they did not comply with the quality criteria)

 Data

P2 (PSIG)

 

P3 (PSIG)

VP (cm3)

 Density (g/cm3) Relative density   Mean relative density
 Run No. 3  17.014 4.149   2.0571  1.2748 1.2748  

1.273 ± 0.001

    
 Run No. 4  17.028 4.152  2.0605  1.2727

1.2727

 Run No. 5  17.077 4.164  2.0600  1.2729 1.2730
Conclusions:
The mean relative density of the test item was D = 1.276 ± 0.003 at 18.7 °C.
Executive summary:

The mean relative density of the test item, which was determined by the pycnometer method according to OECD guideline 109, was D = 1.276 ± 0.003 at 18.7 °C.

Description of key information

The mean relative density of the test item, which was determined by the pycnometer method according to OECD guideline 109, was D = 1.276 ± 0.003 at 18.7 °C.

Key value for chemical safety assessment

Relative density at 20C:
1.276

Additional information