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Diss Factsheets

Physical & Chemical properties

Boiling point

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Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods with acceptable restrictions
Qualifier:
according to guideline
Guideline:
other: ASTM D268
Version / remarks:
Version 31T
Deviations:
not specified
Principles of method if other than guideline:
- Principle of test: not specified
- Short description of test conditions: no data available
GLP compliance:
no
Remarks:
pre-GLP
Type of method:
other: not specified
Specific details on test material used for the study:
TEST MATERIAL:
- Name (as cited): Dichloroethyl ether
- Purity: 99%
Key result
Boiling pt.:
> 172 - < 178 °C
Remarks on result:
other: The atmospheric pressure at which the boiling point was measured is not specified
Conclusions:
The boiling range of Bis(2-chloroethyl) ether was determined to be 172-178°C.
Executive summary:

The boiling range of Bis(2-chloroethyl) ether was determined to be 172-178°C based on ASTM D268-31T. The publication reports the physical properties of various laquer solvents and does not include a detailed description of the methodology or results. However, the estimation of the boiling range of the test substance is based on standard method and the publication has been subject to peer review. It is considered as reliable for assessment (reliability score of 2).

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
- Principle of test: not specified
- Short description of test conditions: no data available
Specific details on test material used for the study:
TEST MATERIAL:
- Names (as cited): Bis(2-chloroethyl) ether
- Purity: not specified
Boiling pt.:
> 175 - < 178 °C
Conclusions:
Bis(2-chloroethyl) ether is described as having a boiling range of 175-178°C.
Executive summary:

According to this recognised handbook, Bis(2-chloroethyl) ether is described as having a boiling range of 175-178°C.

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
supporting study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
data from handbook or collection of data
Principles of method if other than guideline:
- Principle of test: not specified
- Short description of test conditions: no data available
Specific details on test material used for the study:
TEST MATERIAL:
- Names (as cited): 2,2'-Dichloroethyl ether
- Purity: not specified
Boiling pt.:
178.5 °C
Conclusions:
Bis(2-chloroethyl) ether is described as having a boiling point of 178.5°C.
Executive summary:

According to this recongnised databook, the boiling point of Bis(2-chloroethyl) ether is 178.5°C.

Description of key information

Based on ASTM D268-31T, the boiling point of Bis(2-chloroethyl) ether was found to range between 172 and 178°C. The geometric mean of the lower and upper value of the boiling range is reported as key value (i.e. 175°C).

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
175 °C

Additional information

In the published study by Doolittle (Ind. Eng. Chem., 1935, 27(10):1169 -79), the physical properties of various lacquer solvents are provided. Based on ASTM D268-31T (principle of the test method not specified), the boiling point of Bis(2-chloroethyl) ether was found to range between 172 and 178°C. The geometric mean of the lower and upper value of the boiling range is reported as key value (i.e. 175°C). The data published by Doolittle (1930) were obtained based on a standard method and originate from a peer-reeviewed publication. Accordingly, it is considered as reliable and was assigned a reliability score of 2.

Other boiling point / boiling range estimates are available in various handbooks. In the CRC handbook a boiling range of 175-178°C is reported. In Lange's Handbook of Chemistry (15th ed.), Bis(2-chloroethyl) ether is described as having a boiling point equal to 178.8°C. These data are in line with the experimental data reported by Doolittle.