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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-12-24 – 2016-12-24
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
comparable to guideline study
Justification for type of information:
Experimental result performed using standard method of analysis
Qualifier:
according to guideline
Guideline:
other: as mentioned below
Principles of method if other than guideline:
The Freezing point determination of test chemical was done using crushed ice and salt.
GLP compliance:
not specified
Type of method:
other: standard laboratory method
Melting / freezing pt.:
-10.86 °C
Atm. press.:
978.9 hPa
Remarks on result:
other: less than - 10.86 °C

Method Details

Observations

Method

Freezing Temperature Method

-

Principle of Freezing

Point test

The freezing point of a pure sample is the

temperature at which transition from liquid to

solid state takes place at atmospheric

pressure.

-

Quantity of test

item used

g

1 ml

Type of cooling bath used

·        

·        

·        

·        

·        

Crushed Ice- Salt

Type and model no. of temperature sensor used

·        

·        

·        

·        

Thermistor

Atmospheric pressure

hPa

978.9 hPa

Freezing point °C

°C

less than - 10.86 °C

Conclusions:
The Freezing point of test chemical was determined with Freezing Temperature Method and it was determined to be less than -10.86 °C at 978.9 hPa.
Executive summary:

The Freezing point of test chemical was determined with Freezing Temperature Method and it was determined to be less than -10.86 °C at 978.9 hPa.

Description of key information

The Freezing point of test chemical was determined with Freezing Temperature Method and it was determined to be less than -10.86 °C at 978.9 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-10.86 °C

Additional information

The Freezing point determination of test chemical was done using crushed ice and salt . No freezing was observed up to -10.86°C. ence, the freezing point was inferred to be less than -10.86°C at 978.9 hPa.

Other supporting study,the freezing point of test chemical was determined to be less than -60 degree C.

As the data from lab has K1 reliability and the test was performed using standard method of analysis which has the value of freezing point temperature as <-10.86 degree C thus considered as key study for the chemical safety assessment.