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A reaction mixture containing the following components;A. Tetralithium [2(or 3), 9 (or 10), 16 (or 17), 23 (or 24)-tetrakis (3-sulfonato-propylsulfonyl) phthalocyaninato]cupurate (II)B. Trilithium [3-(2-hydroxylpropylsulfamoyl)propylsulfonyl]tris (3-sulfonato-propylsulfonyl)phthalocyaninatocupurate (II)C.Dilithium bis [3-(2-hydroxylpropylsulfamoyl)propylsulfonyl] bis (3-sulfonato-propylsulfonyl)phthalocyaninatocupurate (II)D. Lithium tris [3-(2-hydroxylpropylsulfamoyl)propylsulfonyl] (3-sulfonato-propylsulfonyl)phthalocyaninatocupurate (II)E. Tetrakis [3-(2-hydroxpropylsulfamoyl) proppylsulfonyl]phthalocyaninatocupurate (II)In the ratio A:B:C:D:E 6.25 : 25 : 37.5 : 25 : 6.25
EC number: 472-040-0 | CAS number: -
Vapour pressure
Administrative data
- Endpoint:
- vapour pressure
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- Testing was conducted between 21 March 2005 and 02 June 2005. Report was finalised 15th September 2005.
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: Meets the criteria for classification as Reliable without restriction according to Klimisch et al (1997)
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 005
- Report date:
- 2005
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.4 (Vapour Pressure)
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- dynamic method
Test material
- Test material form:
- solid: particulate/powder
- Remarks:
- migrated information: powder
Constituent 1
Results and discussion
Vapour pressure
- Key result
- Temp.:
- 25 °C
- Vapour pressure:
- < 0 Pa
- Remarks on result:
- other: Less than 7.2 x 10·5 Pa at 25°C
Any other information on results incl. tables
Run 1
| Temp (°C) | Temp (K) | Reciprocal Temp (K-1) | Mass Difference (µg) | Mass Difference (kg) | Vapour Pressure (Pa) | Log10 Vp |
| 230 | 503.15 | 0.001987478 | 11.07 | 1.107E-08 | 0.015367996 | -1.813382758 |
| 231 | 504.15 | 0.001987437 | 11.39 | 1.139E-08 | 0.015812238 | -1.801006655 |
| 232 | 505.15 | 0.001979610 | 9.6 | 9.60E-09 | 0.013327260 | -1.875259146 |
| 233 | 506.15 | 0.001975699 | 11.72 | 1.172E-08 | 0.016270363 | -1.788602767 |
| 234 | 507 .15 | 0.001971803 | 9.03 | 9.03E-09 | 0.012535953 | -1.901842628 |
| 235 | 508.15 | 0.001967923 | 11.88 | 1.188E-08 | 0.016492484 | -1.782713938 |
| 236 | 509.15 | 0.001964058 | 12.12 | 1.212E-08 | 0.016825665 | -1.774027759 |
| 237 | 510.15 | 0.001960208 | 13.02 | 1.302E-08 | 0.018075096 | -1.742919394 |
| 238 | 511 -15 | 0.001956373 | 12.77 | 1.277E-08 | 0.017728032 | -1.751339481 |
| 239 | 512.15 | 0.001952553 | 13.99 | 1.399E-08 | 0.019421704 | -1.711712664 |
| 240 | 513.15 | 0.001952478 | 11.31 | 11.31E-08 | 0.015701178 | -1.804067774 |
Run 2
| Temp (°C) | Temp (K) | Reciprocal Temp (K-1) | Mass Difference (µg) | Mass Difference (Kg) | Vapour Pressure (Pa) | Log10 Vp |
| 230 | 503.5 | 0.001948748 | 9.52 | 1.060E-09 | 0.001471552 | -2.832224513 |
| 231 | 504.15 | 0.001944958 | 10.74 | 1074E+00 | - | - |
| 232 | 505.15 | 0.001941182 | 0.16 | 1.600E-10 | 0.000222121 | -3.653410396 |
| 233 | 506.15 | 0.001937421 | 0.49 | 4.900E-10 | 0.000680246 | -3.167334299 |
| 234 | 507.15 | 0.001933675 | 0.00 | 0.000E+00 | - | - |
| 235 | 508.15 | 0.001929943 | 0.00 | 0.000E+00 | - | - |
| 236 | 509.15 | 0.001926226 | -0.08 | -8.00E-11 | - | - |
| 237 | 510.15 | 0.001922522 | 0.90 | 9.00E-10 | 0.001249431 | -2.903287869 |
| 238 | 511.15 | 0.001918833 | -0.73 | -7.300E-10 | - | - |
| 239 | 512.15 | 0.001915158 | -0.24 | -2.400E-10 | - | - |
| 240 | 513.15 | 0.001911498 | -0.65 | -6.500E-10 | - | - |
Run 3
| Temp (°C) | Temp (K) | Reciprocal Temp (K-1) | Mass Difference (µg) | Mass Difference (Kg) | Vapour Pressure (Pa) | Log10 Vp |
| 230 | 503.15 | 0.001987479 | 8.46 | 8.460E-09 | 0.011744647 | -1.930160016 |
| 231 | 504.15 | 0.001983537 | 7.16 | 7.160E-09 | 0.009939914 | -2.002617356 |
| 232 | 505.15 | 0.001979610 | 8.38 | 8.38E-09 | 0.011633587 | -1.934286360 |
| 233 | 506.15 | 0.001975669 | 5.78 | 5.780E-09 | 0.008024121 | -2.095602540 |
| 234 | 507.15 | 0.001971803 | 7.16 | 7.16E-09 | 0.009939914 | -2.002617356 |
| 235 | 508.15 | 0.001967923 | 7.73 | 7.73E-09 | 0.010731220 | -1.969350885 |
| 236 | 509.15 | 0.001964058 | 8.14 | 8.140E-09 | 0.011300405 | -1.946905974 |
| 237 | 510.15 | 0.001960208 | 6.51 | 6.510E-09 | 0.009037548 | - 2.043949390 |
| 238 | 511.15 | 0.001956373 | 7.97 | 7.970E-09 | 0.011064402 | -1.956072057 |
| 239 | 512.15 | 0.001952553 | 5.29 | 5.290E-09 | 0.007343875 | -2.134074707 |
| 240 | 513.15 | 0.001948748 | 6.27 | 6.2700E-09 | 0.008704366 | -2.060262838 |
Run 4
Temperature (oC) |
Temperature (K) | ReciprocalTemperature(K1) | MassDifference (µg) | MassDifference(kg) |
VapourPressure(Pa) |
Log10Vp | |
230 | 503.15 | 0.001987479 | 6.02 | 6.020E-09 | 0.008357302 | -2.077933887 | |
231 | 504.15 | 0.001983537 | 5.86 | 5.860E-09 | 0.008135181 | -2.089632763 | |
232 | 505.15 | 0.001979610 | 5.37 | 5.370£-09 | 0.007454936 | -2.127556093 | |
233 | 506.15 | 0.001975699 | 5.21 | 5.210E-09 | 0.007232815 | -2.140692655 | |
234 | 507.15 | 0.001971803 | 6.10 | 6.lOOE-09 | 0.008468363 | -2.072200544 | |
235 | 508.15 | 0.001967923 | 5.70 | 5.700E-09 | 0.007913060 | -2.101655523 | |
236 | 509.15 | 0.001964058 | 5.29 | 5.290E-09 | 0.007343875 | -2.134074707 | |
237 | 510.15 | 0.001960208 | 4.64 | 4.640E-09 | 0.006441509 | -2.191012398 | |
238 | 511.15 | 0.001956373 | 4.31 | 4.310E-09 | 0.005983384 | -2.223053109 | |
239 | 512.15 | 0.001952553 | 5.78 | 5.780E-09 | 0.008024121 | -2.095602540 | |
240 |
| 513.15 | 0.001948748 | 5.70 | 5.700E-09 | 0.007913060 | -2.101655523 |
Run 5
Temperature(OC) |
Temperature (K) | ReciprocalTemperature(K1) | MassDifference(µg) | MassDifference(kg) |
VapourPressure(Pa) |
Log10Vp |
230 | 503.15 | 0.001987479 | 3.74 | 3.740E-09 | 0.005192078 | -2.284658777 |
231 | 504.15 | 0.001983537 | 4.15 | 4.150E-09 | 0.005761263 | -2.239482282 |
232 | 505.15 | 0.001979610 | 4.64 | 4.640E-09 | 0.006441509 | -2.191012398 |
233 | 506.15 | 0.001975699 | 4.31 | 4.3lOE-09 | 0.005983384 | -2.223053109 |
234 | 507.15 | 0.001971803 | 4.72 | 4.720E-09 | 0.006552569 | -2.183588380 |
235 | 508.15 | 0.001967923 | 5.13 | 5.130E-09 | 0.007121754 | -2.147413014 |
236 | 509.15 | 0.001964058 | 5.53 | 5.530E-09 | 0.007677057 | -2.114805247 |
237 | 510.15 | 0.001960208 | 3.91 | 3.910E-09 | 0.005428082 | -2.265353621 |
238 | 511.15 | 0.001956373 | 6.43 | 6.430E-09 | 0.008926487 | -2.049319406 |
239 | 512.15 | 0.001952553 | 5.70 | 5.700E-09 | 0.007913060 | -2.101655523 |
240 | 513.15 | 0.001948748 | 5.61 | 5.610E-09 | 0.007788117 | -2.108567517 |
No statistical analysis is given due to the nature of the plot
Applicant's summary and conclusion
- Conclusions:
- The vapour pressure of the test material has been determined to be less than 7 .2 x 10-5 Pa at 25 °C.
- Executive summary:
Introduction:
The Vapour Pressure was measured using EC method 92/69/EEC A4 (vapour pressure balance method)
Results and Conclusions:
The vapour pressure of the test material was determined to be less than 7.2 x 10-6 Pa at 25 °C.
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