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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
20th October 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Remarks:
The thermal Stability of Chemicals by Differential Scanning Calorimetry - ASTM E 537 - 07
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
ASTM E 537 - 07
Deviations:
no
GLP compliance:
not specified
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
14.6 mg of Dioctyldimethylammonium chloride (solvent free). Batch No. 1419598
Key result
Boiling pt.:
>= 176.84 - <= 208.52 °C
Decomposition:
yes
Remarks:
'Before and after boiling point'
Decomp. temp.:
ca. 208.52 °C

Table 1: Phase transition data from DSC curve for 14.6mg'Dioctyldimethylammonium chloride' (solvent free) in temperature program of -30 - 400 °C

(5°C/ min)

   Temperature (°C)  Temperature range (°C)  Enthalpy (J/g)
 Crystallization  -18.74  -24.58 - -18.74 14.93 

 Glass transition

1.01   -6.70 - 1.01 -10.71 
 Melting point 31.32   16.53 - 31.32  -12.84
 Boiling point 208.52   176.84 - 208.52 -841.40 
Conclusions:
The boiling point for the substance is within the range of 176.82 - 208.52 °C with an endpoint of 208.52 °C.
Executive summary:

The substance (dimethyldioctylammonium chloride) boiling point was tested in accordance with ASTM E 537 - 07 (similar, but not directly equivalent to OCED 103). Using Differential Scanning Calorimetry, the boiling point was presented as a range of 176.84 - 208.52 °C with an endpoint of 208.52 °C.

Description of key information

The boiling point for the substance is within the range of 176.82 - 208.52 °C with an endpoint of 208.52 °C.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
208.52 °C

Additional information