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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study according to guideline

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2008
Report date:
2008

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
2-(2-{1-[(2-methoxyphenyl)carbamoyl]-2-oxopropyl}diazen-1-yl)benzoic acid
EC Number:
683-287-0
Cas Number:
877670-90-1
Molecular formula:
C18H17N3O5
IUPAC Name:
2-(2-{1-[(2-methoxyphenyl)carbamoyl]-2-oxopropyl}diazen-1-yl)benzoic acid
Details on test material:
Batch no. 939-76

Results and discussion

Melting / freezing point
Decomposition:
yes
Decomp. temp.:
242 °C

Applicant's summary and conclusion

Conclusions:
In this study Anthranilic Acid-AAOA started to decompose at a temperature of about 242 °C, i.e. 515 K.
Executive summary:

For the determination of the melting point or melting range, the capillary method was used. A small amount of the test item was heated in the electronic controlled sample block and the temperature around the sample was displayed. The sample was observed visually while raising the temperature. The initial and final melting temperatures were determined.

Using a linear heating rate of 0.5 °C/min, Anthranilic Acid-AAOA started to decompose, before the process of melting could be observed.

In this study Anthranilic Acid-AAOA started to decompose at a temperature of about 242 °C, i.e. 515 K.