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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
18 September 2017 to 10 October 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Black viscous liquid
Key result
Decomposition:
no
Remarks on result:
not determinable
Remarks:
no endothermic peak was observed below ambient temperature (substance is a liquid at ambient temperture)

Results of the DSC-measurements

No.

Sample weight / mg

Onset of Effect / °C

Range of effect / °C

Weight loss / mg

Remark

PN14321

24.41

131.38
229.13
285.98

130 – 180 (endo)
220 – 280 (endo)
280 – 330 (endo)

18.54

Figure 1

PN14332

25.48

128.87
221.76
284.78

120 – 210 (endo)
220 – 280 (endo)
280 – 340 (endo)

19.15

Figure 2

During the cooling phase, no thermal effects were observed,which could be assigned to the freezing of the test item.

Conclusions:
No melting/freezing point could be found for the substance
Executive summary:

In a test investigating the melting/freezing point of the substance using differential scanning calometry, no freezing of the substance was seen when temperatures were lowered from ambient to -100°C.

Description of key information

No melting/freezing point could be found for the substance

Key value for chemical safety assessment

Additional information