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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
13 November 2007 to 10 April 2008
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff
Key result
Atm. press.:
1 027 mBar
Decomposition:
yes
Remarks:
the samples were observed to darken above approximately 260°C
Decomp. temp.:
260 °C
Remarks on result:
not determinable
Remarks:
the test substance decomposed at temperatures above approximately 260°C without boiling.

The results of duplicate definitive boiling point determinations on T-13h were as follows: Barometric pressure: 1027 mbar. As the boiling tubes were heated at 1°C/minute, the samples were observed to darken above approximately 260°C, indicating decomposition. No boiling was noted.

Conclusions:
The boiling temperature of T-13h was not determinable, as the test substance decomposed at temperatures above approximately 260°C without boiling.

Description of key information

The boiling temperature of T-13h was not determinable, as the test substance decomposed at temperatures above approximately 260°C without boiling.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
260 °C

Additional information

A boiling point determination was performed as part of a package of physicochemical testing (Huntingdon Life Sciences, 2008, study IDK0104). The boiling point was determined according to OECD Method 103 and EC Method A2, and the study was conducted in compliance with GLP