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Physical & Chemical properties

Flash point

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Reference
Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
20 December 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
The study was conducted according to an internationally recognised method, and under GLP. The test substance is adequately characterised. Therefore full validation applies.
Qualifier:
according to
Guideline:
EU Method A.9 (Flash-Point)
Version / remarks:
2008
Deviations:
no
Qualifier:
according to
Guideline:
ISO 3679 (Determination of flash point - Rapid equilibrium closed cup method)
Version / remarks:
2015
Deviations:
no
Principles of method if other than guideline:
Not applicable
GLP compliance:
yes (incl. certificate)
Remarks:
Inspected on 4,5 and 6 July 2016/ Signed on 10 January 2017
Type of method:
equilibrium method closed cup
Flash point apparatus:
Setaflash apparatus
Key result
Flash point:
ca. 154.5 °C
Atm. press.:
101.3 kPa

First determination:

The flash point of the test item was estimated at 154°C during the first determination. An automatic correction was applied to the obtained result because the ambient pressure was not 101.3 kPa but 99.5 kPa. With this correction, the flash point value was 154.5°C at 101.3 kPa.

Second determination:

The flash point was detected at 154.0°C and the same automatic correction was applied because the ambient pressure was still 99.4 kPa. With this correction, the flash point value was 154.5°C at 101.3 kPa.

Control of the performance of the method:

-         A flash point of 193.5°C was registered for the reference substance glycerol (Batch N° 16H084105)

-         A flash point of 75.5°C was registered for the Certified Reference Material (Batch N° 1151709)

Conclusion:

The corrected flash point of the test item was determined to be 154.5°C at 101.3 kPa (lowest value of two independent determinations).

Interpretation of results:
GHS criteria not met
Conclusions:
The corrected flash point of the test item was determined to be 154.5°C at 101.3 kPa (lowest value of two independent determinations).
Executive summary:

The study was performed in order to determine the flash point of test item according to EU A.9 guideline, using an equilibrium method with closed cup.

The flash point of the test item was determined to be 154.5°C at 101.3 kPa (lowest value of two independent determinations).

The test item is NOT classified as flammable liquid according to Regulation (EC) 1272/2008 (CLP regulation) and UN Globally Harmonised System (GHS).

Description of key information

The flash point of test item was determined to be 154.5°C at 101.3 kPa.

Test item is NOT classified as flammable liquid according to Regulation (EC) 1272/2008 (CLP regulation) and UN Globally Harmonised System (GHS).

Key value for chemical safety assessment

Flash point at 101 325 Pa:
154.5 °C

Additional information

A fully reliable experimental study, conducted according to EU A9 guideline is available.

It is considered as a key study, and the result is retained as key data.