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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
surface tension
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental starting date: 28 April 2017; Experimental completion date: 03 November 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 115 (Surface Tension of Aqueous Solutions)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.5 (Surface Tension)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
ring method

Test material

Constituent 1
Chemical structure
Reference substance name:
Disodium 3,3'-[carbonylbis[imino(3-methoxy-4,1-phenylene)azo]]bis[benzenesulphonate]
EC Number:
233-316-4
EC Name:
Disodium 3,3'-[carbonylbis[imino(3-methoxy-4,1-phenylene)azo]]bis[benzenesulphonate]
Cas Number:
10114-86-0
Molecular formula:
C27H22N6Na2O9S2
IUPAC Name:
disodium 3,3'-[carbonylbis[imino(3-methoxy-4,1-phenylene)azo]]bis[benzenesulphonate]
Test material form:
solid: particulate/powder
Details on test material:
Identification: CIM-42(Direct Yellow 132)
Appearance/physical state: dark orange colored powder
Batch: 161011K
Purity: 94.0%
Expiry / Retest date: 01 December 2017
Storage conditions: Room temperature, in the dark over silica

Results and discussion

Surface tension
Key result
Surface tension:
72.5 mN/m
Temp.:
20 °C
Conc.:
1 g/L
Remarks on result:
other: not surface-active

Any other information on results incl. tables

The readings, times and temperatures for the sample solutions are shown in the following tables:

Table: Sample 1

Age of Solution (mins)

Reading (mN/m)

Temperature (°C)

71

72.5

20.2

80

72.5

20.4

88

72.5

20.4

97

72.5

20.4

105

72.5

20.4

Table : Sample 2

Age of Solution (mins)

Reading (mN/m)

Temperature (°C)

142

72.5

20.4

150

72.5

20.4

159

72.5

20.4

168

72.5

20.4

176

72.5

20.4

Mean Sample 1 result :          72.5mN/m                 pH of Sample 1 :        5.8
Mean Sample 2 result :          72.5mN/m                 pH of Sample 2 :        5.8
Mean result                :          72.5mN/m
Overall temperature   :          20.0 ± 0.5ºC

Applicant's summary and conclusion

Conclusions:
The mean surface tension of duplicate aqueous solutions of test item prepared at 1.0 g/L was determined to be 72.5 mN/m at 20.0 ± 0.5 °C. The test item was considered not to be surface-active.
Executive summary:

72.5mN/m (mean result from duplicate 1.0 g/L aqueous solutions) at 20.0 ± 0.5 °C, using a ring method designed to be compatible with Method A.5 Surface Tension of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 115 of the OECD Guidelines for Testing of Chemicals, 27 July 1995. 

The test item was considered not to be surface-active.