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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes (incl. QA statement)
Type of method:
thermal analysis

Test material

Constituent 1
Test material form:
solid: particulate/powder
Remarks:
migrated information: powder
Details on test material:
Name of test material (as cited in study report): (1 , 1'-Biphenyl) -2-amine,3',4', 5'-trifluoro-
Physical state: solid
Analytical purity: 100.0 % (1H-NMR, see characterization study no. 15L00258)
BASF SE, D-67056 Ludwigshafen
Lot/batch No.: SK03/186
Expiration date of the lot/batch:Mar 22, 2015
Storage condition of test material:Room temperature, protection against humidity

Results and discussion

Melting / freezing point
Melting / freezing pt.:
69 °C
Atm. press.:
1 013 hPa

Any other information on results incl. tables

Results in detail

The melting temperature of the test item was found at 69 °C onset temperature in the 2nd heating.

Determination

Onset temperature

[°C]

Peak temperature

[°C]

A

68.8

70.6

B

68.8

70.7

Mean value

69

71

Observed thermic processes

This observation was confirmed by the preliminary TG/DSC-Test (non-GLP).

In addition to this, an endothermic peak starting at about 150 °C with a weight loss of 100 % at 250 °C showed the vaporization of

the test item.

Applicant's summary and conclusion