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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
The study was conducted between 03 September 2014 and 09 June 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
GLP guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point

Test material

Constituent 1
Chemical structure
Reference substance name:
Amines, C12-14-tert-alkyl, isooctyl mono phosphates
IUPAC Name:
Amines, C12-14-tert-alkyl, isooctyl mono phosphates
Constituent 2
Reference substance name:
Unknown, including minor amounts of diphosphate species, water. Possibly residual unreacted starting material and unknown byproducts.
IUPAC Name:
Unknown, including minor amounts of diphosphate species, water. Possibly residual unreacted starting material and unknown byproducts.
Test material form:
liquid: viscous

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
>= -6 - <= 0 °C

Any other information on results incl. tables

Preliminary Test

The pour point of the preliminary test was -5 ± 3 °C (268 ± 3 K).

 

Main Test

The results are shown in the following table.

 

Determination 1

Determination 2

Stationary point (°C)

-6

-6

Pour point (°C)

-3

-3

Overall pour point result: -3 ± 3 °C (270 ± 3 K)

Applicant's summary and conclusion

Conclusions:
The pour point of the test item has been determined to be -3 ± 3 °C (270 ± 3 K).
Executive summary:

The melting / freezing point of the test substance was -3 ± 3 °C (270 ± 3 K), using the pour point method, designed to be compatible with Method A1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.