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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
March 03, 2015 - March 04, 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
> 500 °C
Atm. press.:
ca. 1 017 hPa
Decomposition:
no
Conclusions:
Boiling Point >500°C
Executive summary:

The determination of the boiling point / boiling range was carried out by differential scanning calorimetry (DSC). The test item and the reference are heated up at a constant heating rate (10 K/min) in a defined atmosphere (nitrogen). Aluminium crucibles with a small hole are used as containers for the test item and as empty reference crucible. The quantity of heat absorbed or released is measured and recorded.

 

The study was performed in accordance with the following guidelines:

EU Method A.2 (Boiling Temperature)

OECD Guideline 103 (Boiling point/boiling range)

 

Results

One DSC measurement in an aluminium crucible with a hole showed no thermal effect in the temperature range of 25 – 500 °C.

After the DSC measurement with the final test temperature of 500 °C the sample in the aluminium crucible appeared unchanged.

The test item had no boiling point within the measurement range of 25 - 500 °C.

 

Boiling Point >500°C

Description of key information

Key value could not be determined in a laboratory study carried out by differential scanning calorimetry (DSC) performed in accordance with OECD Guideline 103 and EU Method A.2.

 

The test item had no boiling point within the measurement range of 25 - 500 °C.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
500 °C

Additional information

The determination of the boiling point / boiling range was carried out by differential scanning calorimetry (DSC).

One DSC measurement in an aluminium crucible with a hole showed no thermal effect in the temperature range of 25 – 500 °C.

After the DSC measurement with the final test temperature of 500 °C the sample in the aluminium crucible appeared unchanged.

The test item had no boiling point within the measurement range of 25 - 500 °C.

Boiling Point >500°C