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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2007
Report date:
2007

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
473-070-7
EC Name:
-
Cas Number:
117428-95-2
Molecular formula:
C12 H13 Cl O3
IUPAC Name:
methyl (2E)-2-[2-(chloromethyl)phenyl]-3-methoxyprop-2-enoate
Details on test material:
-Purity: not reported
Specific details on test material used for the study:
Substance name: Intermediate 5B
Lot #: 50216
Purity: Not reported

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
365 K
Remarks on result:
other: Mean melting temperature: 365 ± 0.5 К or 92.1°C

Applicant's summary and conclusion

Conclusions:
The melting/freezing temperature of the test substance has been determined to be 365 ± 0.5 K.
Executive summary:

Mean melting temperature is 365 ± 0.5 K or 92.1°C by differential scanning calorimetry, using ASTM E537-86, Method A1 of Commission Directive 92/69/EEC.