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Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Deviations:
yes
Remarks:
See details bellow
Principles of method if other than guideline:
Due to the nature of the sample, boiling point was determined by thermogravimetric analysis (TGA), which is a deviation from OECD Guidelines for The Testing of Chemicals, 103, July 27 1995.
Using thermogravimetric analysis, the sample is placed in a DSC hermetic pan with a laser drilled pinhole in the lid. When the sample starts to boil, the vapor pressure in the pan increases causing a weight loss through the pinhole in the lid. The onset of the derivative of this weight loss is taken to be the boiling point of the sample.
GLP compliance:
yes (incl. QA statement)
Type of method:
other: Static method
Boiling pt.:
> 253 - < 254 °C
Atm. press.:
101.3 hPa
Conclusions:
Boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 4,4'-methylenebis(cyclohexylamine) was determined to be 254°C by thermogravimetric analysis (TGA).
Executive summary:

Thermogravimetric analysis (TGA) was used to determine boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 4,4'-methylenebis(cyclohexylamine). The first boiling point of the sample is 254°C.There are two boiling peaks above this temperature however the sample may be decomposing while boiling at the higher temperatures. To be conservative the lowest boiling component is reported as the boiling point of the sample.

Description of key information

Boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 4,4'-methylenebis(cyclohexylamine) was determined to be 254°C by thermogravimetric analysis (TGA).

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
254 °C

Additional information