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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Deviations:
no
GLP compliance:
yes

Test material

Constituent 1
Chemical structure
Reference substance name:
N,N,N',N',N'',N''-hexamethyl-4,4',4''-methylidynetrianiline
EC Number:
210-043-9
EC Name:
N,N,N',N',N'',N''-hexamethyl-4,4',4''-methylidynetrianiline
Cas Number:
603-48-5
Molecular formula:
C25H31N3
IUPAC Name:
4-{bis[4-(dimethylamino)phenyl]methyl}-N,N-dimethylaniline
Test material form:
solid: particulate/powder
Details on test material:
- Purity: 99.4%

Results and discussion

Relative self-ignition temperature (solids)
Key result
Remarks on result:
no self ignition observed under the test conditions

Applicant's summary and conclusion

Conclusions:
Self-ignition was not observed.
Executive summary:

The test was conducted to provide preliminary information on the auto-flammability of solid substances at elevated temperatures in accordance with the procedure described in EU Regulation (EC) 440/2008, Annex Part A test A16.

 

The relative self-ignition temperature test for solids was performed in a temperature programmed oven of approximately 2 litres volume with natural air circulation. A stainless steel wire mesh, 20 mm test cube with 0.045 mm openings was filled with the test sample. The cube is then gently tapped and refilled until completely full. The sample temperature was monitored by a thermocouple placed in the centre of the test cube. Another thermocouple was placed between the test cube and the oven wall to monitor oven temperature. The temperature of the oven and the sample were continuously recorded while the temperature of the oven was increased to 400°C or to the melting point of the solid, if lower, at a rate of 0.5°C/min. The temperature of the oven at which the sample temperature reaches 400°C by self-heating is called the self-ignition temperature.

 

Self-ignition was not observed.