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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
flash point of flammable liquids
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental Starting Date: 30 September 2014 Experimental Completion Date: 22 October 2014
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: see 'Remark'
Remarks:
Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of the relevant results. The study report was conclusive, done to a valid guideline and the study was conducted under GLP conditions.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2014
Report date:
2014

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.9 (Flash-Point)
Deviations:
no
GLP compliance:
yes
Type of method:
equilibrium method closed cup

Test material

Constituent 1
Reference substance name:
NACET00502
IUPAC Name:
NACET00502
Constituent 2
Reference substance name:
119464-63-0 (planar)
IUPAC Name:
119464-63-0 (planar)
Test material form:
other: Clear colorless liquid
Details on test material:
Common/Commercial Name: NACET00502
Chemical Name: 3-methyl-5-((1R)-2,2,3-trimethylcyclopentyl)pentane-2-one
CAS Number: 119464-63-0 (planar)
Appearance/Physical State: Clear colorless liquid
Batch: S-13-11-1
Purity: 98.5%
Expiry Date: 24 December 2015
Storage Conditions: Room temperature in the dark

Results and discussion

Flash point
Flash point:
120 °C
Atm. press.:
101.7 kPa

Any other information on results incl. tables

Results

Results of the flash point determination are shown in the following table.

 

Table 3.1

 

Temperature (ºC)

Observations

23.0

No flash.

28.0

No flash.

33.0

No flash.

38.0

No flash.

43.0

No flash.

48.0

No flash.

53.0

No flash.

58.0

No flash.

63.0

No flash.

68.0

No flash.

73.0

No flash.

73.0 (fresh sample)

No flash.

78.0

No flash.

83.0

No flash.

88.0

No flash.

93.0

No flash.

98.0

No flash.

103.0 (fresh sample)

No flash.

108.0

No flash.

113.0

No flash.

118.0

No flash.

123.0

A blue flash spread across the sample cup.

123.0 (fresh sample)

A blue flash spread across the sample cup.

118.0 (fresh sample)

No flash.

119.0 (fresh sample)

No flash.

120.0 (fresh sample)

A blue flash spread across the sample cup.

120.0 (fresh sample)

A blue flash spread across the sample cup.

118.0 (fresh sample)

No flash.

118.0 (fresh sample)

No flash.

 

Atmospheric pressure = 101.7 kPa

Corrected flash point = 119.9 ºC

Applicant's summary and conclusion

Conclusions:
The flash point of the test item has been determined to be 120 ± 2 °C.
Executive summary:
The determination was carried out using a closed cup flash point tester*, using a procedure designed to be compatible with Method A9 Flash Point of Commission Regulation (EC) No 440/2008 of 30 May 2008.

 

Instrument: Setaflash 30000-0 flash point tester


*Based on, Anon (1983) Paints, Varnishes, Petroleum and Related Products – Determination of Flash Point – Rapid Equilibrium Method,International Standard ISO 3679-2004 (E),Second Edition –2004-04-01,P1-18and Anon (1989) Flash Point of Liquids by Setaflash Closed-Cup Apparatus,ASTM D-3278-89,P1-7.

Conclusion

The flash point of the test item has been determined to be 120 ± 2 °C.