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Physical & Chemical properties

Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
28 March 2017 - 26 May 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Identification: C.I. Solvent Yellow 175 Solid
Batch: ZA07202016
Purity: >99%
Expiry date: 18 July 2019
Storage conditions: room temperature in the dark
Key result
Atm. press.:
101.4 kPa
Decomposition:
yes
Decomp. temp.:
200 °C
Remarks on result:
other: The test item has been determined to decompose from approximately 200 °C (473 K).

The thermographic data for Determinations 1 and 2 are shown in the following table:

    Approximate Temperature (°C)
 Thermal Event  Interpretation  Determination 1 Determination 2 
 exotherm  decomposition  200  200

Atmospheric pressure             :          101.4 kPa

After heating, the samples had lost approximately 42% and 46% of their original weight for Determinations 1 and 2 respectively.

Result: decomposition from approximately 200 °C (473 K).

Due to the low enthalpy change at the onset of decomposition the temperature can only be approximated. The decomposition temperature has been reported as approximately that of the start of the rise in the baseline of the thermograms.

Conclusions:
The test item has been determined to decompose from approximately 200 °C (473 K).
Executive summary:

Boiling Point. Decomposed from approximately 200°C (473 K) at 101.4 kPa by differential scanning calorimetry, designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Description of key information

Boiling Point. Decomposed from approximately 200°C (473 K) at 101.4 kPa by differential scanning calorimetry, designed to be compatible with Method A.2 Boiling Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 103 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Key value for chemical safety assessment

Additional information