Registration Dossier
Registration Dossier
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EC number: 274-159-1 | CAS number: 69852-45-5
Auto flammability
Administrative data
Link to relevant study record(s)
- Endpoint:
- auto-ignition temperature (liquids)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- The study was conducted between 26 May 2016 and 01 June 2016
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.15 (Auto-Ignition Temperature (Liquids and Gases))
- Version / remarks:
- 30 May 2008
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Specific details on test material used for the study:
- SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: Sponsor Batch No. AAE1131000
- Expiration date of the lot/batch: 27 July 2018
STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Room teperature in the dark - Key result
- Auto-ignition temperature:
- > 255 - < 265 °C
- Atm. press.:
- > 100.8 - < 102.2 kPa
- Conclusions:
- The test item has been determined to have an auto-ignition temperature of 260 ± 5 °C.
- Executive summary:
The hazardous physico-chemical properties of 3-[[3-(Dimethylamino)propyl]amino]propanenitrile (TK2710) have been determined. The results are summarized below:
Auto-Ignition Temperature (Liquids and Gases). 260 ± 5 °C, using a procedure designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
Reference
Table 1 Results of auto-ignition temperature determination
Test
temperature (ºC) Test volume (μL) Ignition delay (s) Observations
200 (clean flask) 70 >300 No ignition. Grey fumes were emitted.
250 (clean flask) 70 >300 No ignition. Grey fumes were emitted.
300 (clean flask) 70 2 An orange flame. Grey fumes were emitted. 290 70 3 An orange flame. Grey fumes were emitted. 280 70 5 An orange flame. Grey fumes were emitted. 270 70 7 An orange flame. Grey fumes were emitted. 260 70 >300 No ignition. Grey fumes were emitted.
262 70 >300 No ignition. Grey fumes were emitted.
264 (clean flask) 70 18 An orange flame. Grey fumes were emitted.
262 (clean flask) 70 >300 No ignition. Grey fumes were emitted.
262 (clean flask) 200 27 An orange/blue flame. Grey fumes were emitted.
260 (clean flask) 200 32 An orange/blue flame. Grey fumes were emitted.
258 (clean flask) 200 >300 No ignition. Grey fumes were emitted.
258 (clean flask) 400 >300 No ignition. Grey fumes were emitted.
258 (clean flask) 600 >300 No ignition. Grey fumes were emitted.
258 (clean flask) 800 >300 No ignition. Grey fumes were emitted.
258 (clean flask) 1000 >300 No ignition. Grey fumes were emitted.
Description of key information
The auto-ignition temperature of Aradur 1019 was determined to be 260 +/-0.5°C following a procedure designed to be compatible with Method A.15 Auto-Ignition Temperature (Liquids and Gases) of Commission Regulation (EC) No 440/2008 of 30 May 2008.
Key value for chemical safety assessment
- Autoflammability / Self-ignition temperature at 101 325 Pa:
- 260 °C
Additional information
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