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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
January 2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
comparable to guideline study with acceptable restrictions
Reason / purpose for cross-reference:
reference to same study
Qualifier:
no guideline followed
Principles of method if other than guideline:
TGA analysis was performed on 3 samples of the substance, up to 1000°C.
GLP compliance:
no
Type of method:
other: thermogravimetric analyses
Key result
Decomposition:
ambiguous
Decomp. temp.:
ca. 600 °C
Remarks on result:
not determinable

TGA curves of all 3 tested batches showed weight loss up to ca. 140 -150°C, and then an effect at approximately 600°C, which was ascribed to decomposition of residual OH and CO3 groups in the structure.

No distinct melting effect was observed, thus it is concluded that the substance has no melting temperature.

Conclusions:
The substance does not melt (up to 500°C).
Executive summary:

TGA analysis was performed on 3 batches of the substance, up to 1000°C. A dynamic rate high resolution program was used to obtain the data (Hi-Res sensitivity 1.0, Ramp 50.00°C/min, resolution 4.0).

Helium gas was used to create an inert atmosphere in all analyses.

In none of the tests a melting effect was observed. From this it is concluded that the substance does not have a melting point.

Description of key information

The substance does not melt (up to 500°C).

Key value for chemical safety assessment

Additional information

Result obtained from TGA tests up to 1000°C, following a similar procedure as described in test guidelines, using a dynamic rate high resolution program (Hi-Res sensitivity 1.0, Ramp 50.00°C/min, resolution 4.0) and an inert atmosphere (Helium).