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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
21/09/2017-31/10/2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
GLP compliance:
yes
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Sample identification : 17.076961.0001
Batch Number:Lot 91602E004 20/06/17
Purity:70% w/w of CAS 7281-04-1 and 30% w/w of CAS 18773-88-1 (stated)
Storage:Store at RT

Sample preparation : The test substance and standard reference material were accurately weighted on the aluminium sample holder then sealed before analysis.
Key result
Boiling pt.:
ca. 106.46 °C
Atm. press.:
ca. 5 kPa
Decomposition:
no
Decomp. temp.:
> 106.46 °C
Key result
Boiling pt.:
ca. 103.21 °C
Atm. press.:
ca. 5 kPa
Decomposition:
no
Decomp. temp.:
> 103.21 °C
Conclusions:
Averaged values of boiling point detected are : transition temperature of 104,84°C (onset temperature), with an offset temperature of 113,60°C, and a ΔH of 159,6 J/g.
Executive summary:

On an OECD 102 study, averaged values of boiling point detected are : transition temperature of 104,84°C (onset temperature), with an offset temperature of 113,60°C, and a ΔH of 159,6 J/g.

Description of key information

On an OECD 102 study, averaged values of boiling point detected are : transition temperature of 104,84°C (onset temperature), with an offset temperature of 113,60°C, and a ΔH of 159,6 J/g.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
104.84 °C

Additional information