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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2005
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: GLP missing, but test in analogy to official guideline

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2001
Report date:
2001

Materials and methods

Test guideline
Qualifier:
equivalent or similar to guideline
Guideline:
other: national standard (VDI 2263)
Principles of method if other than guideline:
Differential Scanning Calorimetry (DSC)
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
3-hydroxy-N-(o-tolyl)-4-[(2,4,5-trichlorophenyl)azo]naphthalene-2-carboxamide
EC Number:
229-440-3
EC Name:
3-hydroxy-N-(o-tolyl)-4-[(2,4,5-trichlorophenyl)azo]naphthalene-2-carboxamide
Cas Number:
6535-46-2
Molecular formula:
C24H16Cl3N3O2
IUPAC Name:
3-hydroxy-N-(2-methylphenyl)-4-[(2,4,5-trichlorophenyl)diazenyl]-2-naphthamide
Test material form:
solid: nanoform, no surface treatment

Results and discussion

Melting / freezing point
Atm. press.:
ca. 1 013
Decomposition:
yes
Decomp. temp.:
270 °C
Remarks on result:
other: decomposition with a mean energy of -300 J/g

Any other information on results incl. tables

Closed cup: The measurements showed an endothermic effect in the temperature range 260 - 270°C directly followed by a spontaneous exothermal decomposition in the temperature ranges 270 - 290°C with a decomposition energy of -170 J/g followed by a second exothermal decomposition in the temperature ranges 290 - 450°C with a decomposition energy of -300 J/g.

Open cup: A measurement showed an oxidation reaction starting at approximately 240°C. This oxidation reaction covers the thermal decomposition.

Applicant's summary and conclusion