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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Remarks:
GLP and appropriate guidelines
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Deviations:
no
Principles of method if other than guideline:
n/a
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature

Test material

Constituent 1
Chemical structure
Reference substance name:
Diethyl (hydroxymethyl)phosphonate
EC Number:
221-391-6
EC Name:
Diethyl (hydroxymethyl)phosphonate
Cas Number:
3084-40-0
Molecular formula:
C5H13O4P
IUPAC Name:
diethyl (hydroxymethyl)phosphonate
Constituent 2
Reference substance name:
Diethoxyphosphoryl methanol
IUPAC Name:
Diethoxyphosphoryl methanol
Test material form:
other: "medium viscosity" liquid
Details on test material:
E06-16 (Lot No. 1041-37-6, T# 184), a colotless liquid. Stored in dark at room temp. (Approximately 25oC).
The test material was stable for the duration of the study.

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
-34 °C
Atm. press.:
1 013.25 hPa

Any other information on results incl. tables

A freezing point according to the criteria of the guidelines could not be determined down to – 40 °C. No typical observation concerning a phase transition was observed. At the end of the measurement the test item was liquid.

Applicant's summary and conclusion

Conclusions:
The freezing point of E06-16 is -34oC at normal atmospheric pressure.
Executive summary:

The freezing point of E06-16 is -34oC.