N-acetylsulphanilyl chloride

Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Justification for type of information:

Experimental test result performed using standard OECD test guidelines

Qualifier:

according to guideline

Guideline:

OECD Guideline 103 (Boiling point/boiling range)

GLP compliance:

no

Type of method:

method according to Siwoloboff

Key result

Boiling pt.:

> 300 °C

Atm. press.:

97 510 Pa

Decomposition:

no

Remarks on result:

other: Other details not available

Observation table & Result :

Method Details		Observations	Remarks if, any
Guideline	OECD 103
Method	Method according to Siwoloboff
Principle of Boiling point test	A sample is heated gradually in a tube which is immersed in a liquid bath. The sample tube is held in close contact with a thermometer and it contains a boiling capillary which is fused about 1 cm above its lower end. Upon approach of the boiling temperature bubbles emerge rapidly from the lower open end of the capillary. The boiling temperature is that temperature at which, on momentary cooling, the string of bubbles stops and liquid suddenly rises in the capillary.		no string of bubbles were observed upto 300 °C inferring boiling point to be greater than 300°C
Volume of chemical used	ml/ g	1 g	-
Nature of the Bath taken	·    Oil bath ·    Water bath	Oil bath	-
	If oil bath is used, the type of oil ·    Liquid paraffin ·    Silicone oil	Silicon oil	-
Atmospheric pressure	hPa	975.1 hPa	-
Decomposition	Decomposition temperature (°C), if applicable ·                    Yes ·                    No	No	-
Boiling point (°C) (RESULT)	°C	> 300°C	-
Boiling point range, if applicable	°C	-	-

Conclusions:

The boiling point determination of test substance was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical was determined to be > 300°C at 97510 Pa

Executive summary:

The boiling point determination of test substance was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical was determined to be > 300°C at 97510 Pa

Description of key information

On the basis of datafrom study report,the boiling point determination of test substance was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical was determined to be > 300°C at 97510 Pa.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:

300 °C

Additional information

On the basis of datafrom study report,the boiling point determination of test substance was done as per the test guideline OECD 103. The method followed was according to Siwoloboff. The boiling point of test chemical was determined to be > 300°C at 97510 Pa.

In a supporting study from modelling database, EPI Suite MPVPBP V1.43 was used to predict the boiling point of test chemical. The boiling point of chemical was evaluated to be 405.54˚C

Additional study from authoritative and modelling database indicates the boiling point of test chemical as 426.8±28.0 °C at 101325 Pa.