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Diss Factsheets

Physical & Chemical properties

Density

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Reference
Endpoint:
relative density
Type of information:
experimental study
Adequacy of study:
key study
Study period:
This study was conducted between 19 December 2016 and 25 May 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Information is derived from a reliable in-house study according to OECD TG 109 using the gas comparison pycnometer method.
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Version / remarks:
02 October 2012
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.3 (Relative Density)
Version / remarks:
EC No. 440/2008 of 30 May 2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
air comparison pycnometer (for solids)
Specific details on test material used for the study:
Identification : 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with ethylenediamine
Appearance/Physical state: Yellow/brown extremely viscous liquid
Batch : BBF01102V1
Purity : 100% UVCB
Expiry date : 01 January 2021
Storage conditions*: Room temperature in the dark

* Test item was held at room temperature in the dark, heated to approximately 50 or 80 °C for subsampling, as per sponsor’s communications.
Key result
Type:
relative density
Density:
ca. 1.22 other:
Temp.:
20 °C
Key result
Type:
density
Density:
ca. 1 220 kg/m³
Temp.:
20 °C

Sample Results


The pressure readings and volumes obtained for the vessel and the vessel containing the test item are shown in the following table:


















































































Use



Determination



P1


(psig)



P2


(psig)



P3


(psig)



P4


(psig)



Reference


Cell Volume (cm3)



Sample


Cell Volume (cm3)



Empty Vessels



1



17.317



6.554



17.828



8.835



90.593



148.772



2



18.441



6.994



17.741



8.805



90.959



148.871



3



18.115



6.876



17.596



8.729



91.413



149.418



Mean



90.988



149.020



Vessel and Test Item



4



17.092



6.470



17.637



8.738



90.740



148.971



5



17.691



6.699



17.692



8.762



90.979



149.283



6



17.785



6.741



18.086



8.958



91.319



149.611



Mean



91.013



149.288



 


Sample


The pressure readings and volumes obtained for the vessel and the vessel containing the test item are shown in the following table:












































































Determination



Test



Vessel



Vessel and Test Item



P1(sample)
(psig)



P2(sample)
(psig)



Volume
(cm3)



P3(sample)
(psig)



P4(sample)
(psig)



Volume
(cm3)



1



A



17.441



7.029



14.240



17.316



7.925



41.439



B



17.795



7.165



14.030



17.916



8.199



41.425



C



17.469



7.032



13.974



17.586



8.048



41.425



2



A



17.775



7.171



14.473



17.721



8.300



45.983



B



17.461



7.038



14.270



17.918



8.392



45.977



C



17.821



7.182



14.235



17.890



8.377



45.933



The calculated mean volumes and densities are shown in the following table:



























Determination



Mean Volume
of Vessel
(cm3)



Mean Volume
of Vessel and
Test Item (cm3)



Volume of
Test Item
(cm3)



Density


(kg/m3)



1



14.081



41.430



27.348



1.151 x 103



2



14.326



45.964



31.638



1.149 x 103



Mean density:            1.15x 103kg/m3


Relative density:        1.15


Temperature:              19.0 ± 1.0 ºC

Conclusions:
The density of the test item was determined to be 1.15 x 10^3 kg/m3 at 19.0 ± 1.0 ºC. The corresponding relative density was calculated to be 1.15.
Executive summary:

The general physico-chemical properties of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with ethylenediamine have been determined.

Density. 1.15 x 103kg/m3at19.0 ± 1.0 ºC. The corresponding relative density was calculated to be 1.15, using a gas comparison pycnometer, designed to be compatible with Method A.3 Relative Density of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 109 of the OECD Guidelines for Testing of Chemicals, 02 October 2012.

Description of key information

Key value for chemical safety assessment

Relative density at 20C:
1.15

Additional information