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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016-05-18
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Key result
Atm. press.:
ca. 101 325 Pa
Decomposition:
yes
Remarks:
The substance appeared brown at approx. 300 °C and started to decompose at about 330 °C.
Decomp. temp.:
ca. 330 °C

Testing the control substance caffeine (mean melting temperature of 236.1 °C) confirmed the reliability of the apparatus.

Conclusions:
As the substance decomposed at approx. 330 °C, no melting point could be determined.
Executive summary:

The melting point of the substance was investigated in an experimental study under GLP conditions according to OECD Test Guideline 102 using the capillary method. As the substance decomposed at approx. 330 °C, no melting point could be determined.

Description of key information

As the substance decomposed at approx. 330 °C, no melting point could be determined (reference 4.2-1).

Key value for chemical safety assessment

Additional information

The melting point of the substance was investigated in an experimental study under GLP conditions according to OECD Test Guideline 102 using the capillary method. As the substance decomposed at approx. 330 °C, no melting point could be determined.