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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
not specified
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential thermal analysis
Key result
Decomposition:
yes
Decomp. temp.:
ca. 347 °C

Differential thermal analysis (DTA):

1,10-Decanediamine, 4-methylbenzenesulfonate (1:2) was heated up from the starting temperature to the final temperature at a constant heating rate in a defined atmosphere. Endothermal or exothermal effects were measured and recorded.

The DTA measurement showed a first endothermal effect at approximately 138 °C, which is interpreted to be the presumed melting point of the substance.

A second endothermal effect was observed at approximately 347 °C. After the measurement, the test item was discoloured to black. Therefore this second effect is interpreted to be the initial boiling point accompanied by the decomposition of the substance.

Conclusions:
1,10-Decanediamine, 4-methylbenzenesulfonate (1:2) has no boiling point at atmospheric pressure. Boiling accompanied by decomposition of the substance start at approximately 347 °C.
Executive summary:

This study following EU Method A.2 (Boiling temperature) is considered suitable for use as key study for this endpoint. The boiling point /boiling range of 1,10-Decanediamine, 4-methylbenzenesulfonate (1:2) was determined by differential thermal analysis.

1,10-Decanediamine, 4-methylbenzenesulfonate (1:2) has no boiling point at atmospheric conditions.

Boiling accompanied by decomposition of the substance starts at approximately 347 °C.

Description of key information

1,10-Decanediamine, 4-methylbenzenesulfonate (1:2) has no boiling point at atmospheric pressure. Boiling accompanied by decomposition of the substance starts at approximately 347 °C.

Key value for chemical safety assessment

Additional information

A study (Boiling point Currenta 2018) following EU Method A.2 (Boiling temperature) was performed to determine the boiling point of 1,10-Decanediamine, 4-methylbenzenesulfonate (1:2)

It was concluded that the test item has no boiling point at atmospheric conditions as boiling accompanied by the decomposition of the substance starts at approximately 347 °C.