Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
(EC) No 440/2008 A.2
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: DIN 53171 Solvents for paints and varnishes - Determination of destination characteristics
Deviations:
not specified
GLP compliance:
yes (incl. QA statement)
Type of method:
distillation method

Test material

Constituent 1
Chemical structure
Reference substance name:
4-cyclohexylphenol
EC Number:
214-465-4
EC Name:
4-cyclohexylphenol
Cas Number:
1131-60-8
Molecular formula:
C12H16O
IUPAC Name:
4-cyclohexylphenol
Test material form:
solid: flakes

Results and discussion

Boiling point
Key result
Boiling pt.:
299 °C
Atm. press.:
1 028 hPa
Decomposition:
no

Applicant's summary and conclusion

Conclusions:
The GLP study was performed according to EU method A.2 without deviations and therefore reliability of Klimisch 1 has been assigned. Boiling point has been determined to be 299°C.
Executive summary:

The boiling point at 299 °C of the test substance was determined in a GLP test according to EU method A.2 using the distillation method. The test item was filled in a distillation flask and heated up until beginning of boiling. Due to the melting point of 128 °C the temperature in the gas-room of the distillation flask was read off, when the vapour front reached the thermocouple in the gas-room and condensed there.

The atmospheric pressure at the time of measurement was 1028 hPa. The temperature of the thermocouple of the gas-room was 300 °C when the vapour began to condensate. The temperature of the liquid was 298 °C at this time. A temperature correction according to Sidney-Young gives a boiling point at normal pressure of 299 °C.